Week - 1 |
Distillation techniques |
Week - 2 |
Simple distillation, vacuum distillation |
Week - 3 |
Steam distillation, azeotropic distillation and sublimation |
Week - 4 |
Extraction and separation of solvents |
Week - 5 |
Crystallization techniques, solvent selection |
Week - 6 |
Crystallization techniques, binary and ternary solvent mixtures |
Week - 7 |
Drying techniques and removing the solvents |
Week - 8 |
Introduction to chromatographic methods |
Week - 9 |
Separation and purification by thin layer chromatography |
Week - 10 |
Separation and purification by colon chromatography |
Week - 11 |
Separation and purification by flash chromatography |
Week - 12 |
Separation and purification by preparative HPLC |
Week - 13 |
Resolution of rasemic mixtures |
Week - 14 |
Storage of synthesis products |